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Status of NE-CAT Sector 24 ActivitiesJanuary 2008
APS accelerator operation was shut down for preventative maintenance for the month of January. Consequently there is no beamline user experience to report. The month long shut down presented an opportunity for the NE- CAT staff to perform preventative maintenance on the beamlines as well as introduce new capabilities for the users upon resumption of APS’ user operation in February. The major new capability introduced during the shut down was the installation of a sample placement robotic system on the 24-ID-C variable energy beam line. A photograph of the current installation is shown below.
The robotic system is an originally ALS designed and fabricated system which NE- CAT previously operated on its 8-BM bending magnet beamline. This beamline has been taken out of service and is in the process of being moved to Sector 24. In order to install the robot on to the 24-ID-C beamline extensive modifications were made. The “handedness” of the robot had to be reversed, i.e., looking downstream from the source, the robot had to be installed on the left side of the goniometer rather than the right as was the case of the 8-BM beam line. In performing this change all the electrical wiring and pneumatic tubing were upgraded to provide improved reliability. A new cover for the liquid nitrogen Dewar was also installed to minimize frosting and a gravity-feed liquid-nitrogen delivery system was installed to eliminate turbulence in the liquid nitrogen Dewar containing the samples during automatic filling. The operating software has also been integrated into the beamline data acquisition system. The end result of these many changes is that the robot can now operate unattended for several days mounting and dismounting sample pins hundreds of time without a failure. The first user test of the robot will take place in mid February. If the early user experiences are successful, the robot system will increasingly be scheduled for use by the user community.
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Recent Highlights10/07/2009 *NE-CAT's executive committee member Thomas Steitz shares 2009 Nobel Prize in Chemistry* The Nobel Assembly at the Karolinska Institute in Sweden announced today that Thomas Steitz is one of three winners of the 2009 Nobel Prize in Chemistry for his work describing the structure and function of the ribosome. Thomas Steitz is a member of NE-CAT's executive committee and a frequent user of NE-CAT beamlines. 09/03/2009
Crystal Structure of the ATP-Gated P2X4 Ion Channel in the Closed State, Toshimitsu Kawate, Jennifer Carlisle Michel, William T. Birdsong, and Eric Gouaux, Nature 460, 592-598 (2009) Formation of the First Peptide Bond: the Structure of EF-P Bound to the 70S Ribosome, Gregor Blaha, Robin E. Stanley, and Thomas A. Steitz, Science 325, 966-970 (2009) Structures of the Ribosome in the Intermediate States of Ratcheting, Wen Zhang, Jack A. Dunkle and Jamie H.D. Cate, Science 325, 1014-1017 (2009) 09/02/2009 August 2009 status report now available. 08/06/2009 July 2009 status report now available. 06/30/2009 June 2009 status report now available. 06/18/2009 Looking for Ways to Improve Vaccines Against the Deadly Rotavirus 06/09/2009 May 2009 status report now available. 05/01/2009 April 2009 status report now available. 03/06/2009 February 2009 status report now available. 02/16/2009 New MD2 installed on 24-ID-C beamline with sample placement robot now available to users. 02/09/2009 January 2009 status report now available. 1/23/2009 NE-CAT Resource Advisory Committee Meets. See pic. 1/13/2009 December 2008 Status report available. 12/11/2008 November 2008 Status report available. 11/04/2008 Featured Publication Structure of a complex of the ATPase Sec A and the protein-translocation channel J. Zimmer, Y. Nam & T. Rapoport Nature 455, 936-945 (2008) Click here for full article. NE-CAT’s second MD2 microdiffractometer is delivered. |
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