Structures of RNA phosphotransferase Tpt1 reveal distinct binding modes for an RNA 2'-PO splice junction versus a 5'-PO mononucleotide.

Publication Type:

Journal Article

Source:

RNA, Volume 31, Issue 7, p.916-922 (2025)

Keywords:

Binding Sites, Crystallography, X-Ray, Humans, Models, Molecular, Nucleic Acid Conformation, Protein Binding, RNA, RNA Splicing

Abstract:

<p>Tpt1 is a widely distributed enzyme that removes an internal RNA 2&#39;-phosphate by transfer to NAD, via a two-step reaction in which: (i) the RNA 2&#39;-PO attacks NAD to form an RNA-2&#39;-phospho-(ADP-ribose) intermediate and expel nicotinamide; and (ii) the ADP-ribose O2&Prime; attacks the RNA 2&#39;-phosphodiester to form 2&#39;-OH RNA and ADP-ribose-1&Prime;,2&Prime;-cyclic phosphate products. Tpt1 can also execute a single-step ADP-ribosyltransferase reaction at a 5&#39;-monophosphate nucleic acid terminus that installs a 5&#39;-phospho-ADP-ribose cap structure. Here we present crystal structures of Tpt1 bound to an RNA containing an internal 2&#39;-PO mark (the substrate for the canonical Tpt1 pathway) and in a complex with 5&#39;-AMP. We find that Tpt1 has distinct binding modes, whereby the RNA 2&#39;-PO and the AMP 5&#39;-PO are engaged by the same set of active site amino acids, but the 2&#39;-PO nucleoside and the 5&#39;-nucleoside occupy different sites on the enzyme.</p>

PDB: 
8TG5 and 8TKB
Detector: 
EIGER
Beamline: 
24-ID-E